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Question: Answered & Verified by Expert
In III group precipitation, $\mathrm{NH}_4 \mathrm{Cl}$ is added before adding $\mathrm{NH}_4 \mathrm{OH}$ to
ChemistryChemical EquilibriumJIPMERJIPMER 2009
Options:
  • A decrease conc. of $\mathrm{OH}^{-}$
  • B prevent interference of $\mathrm{PO}_4^{3-}$
  • C increase conc. of $\mathrm{Cl}^{-}$
  • D increase conc. of $\mathrm{OH}^{-}$ion
Solution:
1648 Upvotes Verified Answer
The correct answer is: decrease conc. of $\mathrm{OH}^{-}$
In III group precipitation, $\mathrm{NH}_4 \mathrm{Cl}$ is added before adding $\mathrm{NH}_4 \mathrm{OH}$ to decrease the conc. of$\mathrm{OH}^{-}$, as $\mathrm{NH}_4 \mathrm{Cl}$ and $\mathrm{NH}_4 \mathrm{OH}$ dissociates as follows.
$\begin{aligned}
& \mathrm{NH}_4 \mathrm{Cl} \rightleftharpoons \mathrm{NH}_4^{+}+\mathrm{Cl}^{-} \\
& \mathrm{NH}_4 \mathrm{OH} \rightleftharpoons \underset{\substack{\text { common } \\
\text { ion }}}{\mathrm{NH}_4^{+}+\mathrm{OH}^{-}}
\end{aligned}$
Due to presence of common ion, conc. of $\mathrm{OH}^{-}$ decreases and for III group precipitation lesser conc. of $\mathrm{OH}^{-}$is required.

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